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Optical, mechanical and fractographic response of transparent alumina ceramics on erbium doping

机译:transparent掺杂透明氧化铝陶瓷的光学,机械和分形学响应

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摘要

Alumina ceramics found their utilisation in many applications which can be further extend by attaining functional properties; in our case the transparency obtained through precise processing and photoluminescence due to erbium (Er) doping. In order to examine the optical, mechanical and fractographicresponse of transparent alumina on Er doping, slip casted samples containing 0–0.15 at.% of erbiumnano-oxide were pre-sintered by two-step sintering regime and then hot isostatically pressed. Preparedsamples exhibited fully dense submicron microstructure and corresponding high transparency (RIT upto 60%). Positive influence of doping on the Vickers hardness resulted in values up to 27 GPa (at 10 Nload). Moreover, the comparison of the Vickers hardness determined at different loadings with literaturedata showed that the Er doped alumina is one of the hardest material in this category. The samples werecharacterised also in terms of fracture toughness and fractographic behaviour.
机译:氧化铝陶瓷在许多应用中得到了利用,通过获得功能特性可以进一步扩展。在我们的案例中,由于precise(Er)掺杂,通过精确的加工和光致发光获得的透明性。为了检查透明氧化铝在Er掺杂上的光学,机械和分形反应,将含0-0.15 at。%的氧化二铌的滑模铸造样品通过两步烧结方案进行预烧结,然后进行热等静压。制备的样品显示出完全致密的亚微米微观结构和相应的高透明度(RIT高达60%)。掺杂对维氏硬度的积极影响导致值高达27 GPa(在10 Nload时)。此外,在不同载荷下测定的维氏硬度与文献数据的比较表明,掺Er的氧化铝是该类别中最坚硬的材料之一。样品还具有断裂韧性和断裂形貌特征。

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